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Contents: Introduction, Introduction to Laboratory Work, Measurement by Weight, Measurement by Volume, General Remarks on Volumetric Analysis, Evaluation of Analytical Data, pH and Buffers, Solvent Extraction, General Remarks on Gravimetric Methods of Analysis, Radox Titrations, Precipitation Titrations, Complexometric Titrations, Chromatography, Electroanalytical Techniques.

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Genre: Chemistry, Analytic
Author: S. A. Iqbal
Publisher: Discovery Publishing House
Release: 1994
File: 202 Pages
ISBN-13: 8171412440

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The definitive textbook on the chemical analysis of pharmaceutical drugs ­– fully revised and updated Introduction to Pharmaceutical Analytical Chemistry enables students to gain fundamental knowledge of the vital concepts, techniques and applications of the chemical analysis of pharmaceutical ingredients, final pharmaceutical products and drug substances in biological fluids. A unique emphasis on pharmaceutical laboratory practices, such as sample preparation and separation techniques, provides an efficient and practical educational framework for undergraduate studies in areas such as pharmaceutical sciences, analytical chemistry and forensic analysis. Suitable for foundational courses, this essential undergraduate text introduces the common analytical methods used in quantitative and qualitative chemical analysis of pharmaceuticals. This extensively revised second edition includes a new chapter on chemical analysis of biopharmaceuticals, which includes discussions on identification, purity testing and assay of peptide and protein-based formulations. Also new to this edition are improved colour illustrations and tables, a streamlined chapter structure and text revised for increased clarity and comprehension. Introduces the fundamental concepts of pharmaceutical analytical chemistry and statistics Presents a systematic investigation of pharmaceutical applications absent from other textbooks on the subject Examines various analytical techniques commonly used in pharmaceutical laboratories Provides practice problems, up-to-date practical examples and detailed illustrations Includes updated content aligned with the current European and United States Pharmacopeia regulations and guidelines Covering the analytical techniques and concepts necessary for pharmaceutical analytical chemistry, Introduction to Pharmaceutical Analytical Chemistry is ideally suited for students of chemical and pharmaceutical sciences as well as analytical chemists transitioning into the field of pharmaceutical analytical chemistry.

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Genre: Science
Author: Stig Pedersen-Bjergaard
Publisher: Wiley
Release: 2019-04-22
File: 544 Pages
ISBN-13: 9781119362722

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Genre: Chemistry, Analytic
Author: Douglas A. Skoog
Publisher:
Release: 2011
File: 656 Pages
ISBN-13: 9814272795

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Principles of Analytical Chemistry gives readers a taste of what the field is all about. Using keywords of modern analytical chemistry, it constructs an overview of the discipline, accessible to readers pursuing different scientific and technical studies. In addition to the extremely easy-to-understand presentation, practical exercises, questions, and lessons expound a large number of examples.

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Genre: Science
Author: Miguel Valcarcel
Publisher: Springer Science & Business Media
Release: 2000-08-15
File: 372 Pages
ISBN-13: 354064007X

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Genre: Chemistry, Analytic
Author: John Muter
Publisher:
Release: 1882
File: 216 Pages
ISBN-13: STANFORD:24503282420

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Modern Analytical Chemistry is a one-semester introductory text that meets the needs of all instructors. With coverage in both traditional topics and modern-day topics, instructors will have the flexibilty to customize their course into what they feel is necessary for their students to comprehend the concepts of analytical chemistry.

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Genre: Science
Author: David Harvey
Publisher: McGraw-Hill Science, Engineering & Mathematics
Release: 2000
File: 798 Pages
ISBN-13: 0072375477

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List of figures p. ix List of tables p. xii Preface p. xiii Part I The Role of Analytical Chemistry in Archaeology p. 1 1 Archaeology and Analytical Chemistry p. 3 1.1 The history of analytical chemistry in archaeology p. 5 1.2 Basic archaeological questions p. 10 1.3 Questions of process p. 25 2 An Introduction to Analytical Chemistry p. 31 2.1 What is chemistry? p. 31 2.2 Analytical chemistry p. 38 2.3 Special considerations in the analysis of archaeological material p. 42 Part II The Application of Analytical Chemistry to Archaeology p. 45 3 Elemental Analysis By Absorption and Emission Spectroscopies in the Visible and Ultraviolet p. 47 3.1 Optical emission spectroscopy (OES) p. 47 3.2 Atomic absorption spectroscopy (AAS) p. 48 3.3 Inductively coupled plasma atomic emission spectroscopy (ICP-AES) p. 57 3.4 Comparison of analysis by absorption/emission spectrometries p. 60 3.5 Greek pots and European bronzes - archaeological applications of emission/absorption spectrometries p. 62 4 Molecular Analysis by Absorption and Raman Spectroscopy p. 70 4.1 Optical and UV spectrophotometry p. 70 4.2 Infrared absorption spectroscopy p. 77 4.3 Raman spectroscopy p. 83 4.4 Soils, bone, and the "Baltic shoulder"--Archaeological applications of vibrational spectroscopy p. 85 5 X-ray Techniques and Electron Beam Microanalysis p. 93 5.1 Introduction to X-rays p. 93 5.2 X-ray fluorescence (XRF) spectrometry p. 101 5.3 Electron microscopy as an analytical tool p. 109 5.4 X-ray diffraction p. 113 5.5 Other X-ray related techniques p. 116 5.6 A cornucopia of delights - archaeological applications of X-ray analysis p. 118 6 Neutron Activation Analysis p. 123 6.1 Introduction to nuclear structure and the principles of neutron activation analysis p. 123 6.2 Neutron activation analysis in practice p. 128 6.3 Practical alchemy - archaeological applications of NAA p. 130 7 Chromatography p. 137 7.1 Principles of chromatography p. 137 7.2 Classical liquid column chromatography p. 139 7.3 Thin layer chromatography (TLC) p. 139 7.4 Gas chromatography (GC) p. 142 7.5 High performance liquid chromatography (HPLC) p. 146 7.6 Sticky messengers from the past - archaeological applications of chromatography p. 147 8 Mass Spectrometry p. 160 8.1 Separation of ions by electric and magnetic fields p. 160 8.2 Light stable isotopes (¿D, ¿13C, ¿15N, ¿18O, and ¿34S) p. 169 8.3 Heavy isotopes (Pb, Sr) - thermal ionization mass spectrometry (TIMS) p. 173 8.4 Combined techniques - GC-MS p. 174 8.5 Isotope archaeology - applications of MS in archaeology p. 176 9 Inductively Coupled Plasma-Mass Spectrometry (ICP-MS) p. 195 9.1 Types of ICP analysis p. 195 9.2 Comparison with other techniques p. 200 9.3 Instrument performance p. 202 9.4 Splitting hairs - archaeological applications of ICP-MS p. 208 Part III Some Basic Chemistry for Archaeologists p. 215 10 Atoms, Isotopes, Electron Orbitals, and the Periodic Table p. 217 10.1 The discovery of subatomic particles p. 217 10.2 The Bohr-Rutherford model of the atom p. 227 10.3 Stable and radioactive isotopes p. 230 10.4 The quantum atom p. 238 10.5 The periodic table p. 243 11 Valency, Bonding, and Molecules p. 249 11.1 Atoms and molecules p. 249 11.2 Bonds between atoms p. 253 11.3 Intermolecular bonds p. 258 11.4 Lewis structures and the shapes of molecules p. 260 11.5 Introduction to organic compounds p. 263 11.6 Isomers p. 269 12 The Electromagnetic Spectrum p. 275 12.1 Electromagnetic waves p. 275 12.2 Particle-wave duality p. 279 12.3 Emission lines and the Rydberg equation p. 281 12.4 Absorption of EM radiation by matter - Beer's law p. 286 12.5 The EM spectrum and spectrochemical analysis p. 288 12.6 Synchrotron radiation p. 290 13 Practical Issues in Analytical Chemistry p. 294 13.1 Some basic procedures in analytical chemistry p. 294 13.2 Sample preparation for trace element and residue analysis p. 302 13.3 Standards for calibration p. 306 13.4 Calibration procedures and estimation of errors p. 309 13.5 Quality assurance procedures p. 319 Epilogue p. 322 Appendices p. 326 I Scientific notation p. 326 II Significant figures p. 327 III Seven basic SI units p. 328 IV Physical constants p. 329 V Greek notation p. 330 VI Chemical symbols and isotopes of the elements p. 331 VII Electronic configuration of the elements (to radon, Z=86) p. 335 VIII Some common inorganic and organic sample preparation methods used in archaeology p. 337 IX General safe practice in the laboratory p. 340 X COSHH assessments p. 342 References p. 350 Index.

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Genre: Social Science
Author: A. M. Pollard
Publisher: Cambridge University Press
Release: 2007
File: 404 Pages
ISBN-13: 0521655722

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Analytical Chemistry, Second Edition covers the fundamental principles of analytical chemistry. This edition is organized into 30 chapters that present various analytical chemistry methods. This book begins with a core of six chapters discussing the concepts basic to all of analytical chemistry. The fundamentals, concepts, applications, calculations, instrumentation, and chemical reactions of five major areas of analytical chemistry, namely, neutralization, potentiometry, spectroscopy, chromatography, and electrolysis methods, are emphasized in separate chapters. Other chapters are devoted to a discussion of precipitation and complexes in analytical chemistry. Principles and applications and the relationship of these reactions to the other areas are stressed. The remaining chapters of this edition are devoted to the laboratory. A chapter discusses the basic laboratory operations, with an emphasis on safety. This topic is followed by a series of experiments designed to reinforce the concepts developed in the chapters. This book is designed for introductory courses in analytical chemistry, especially those shorter courses servicing chemistry majors and life and health science majors.

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Genre: Science
Author: Clyde Frank
Publisher: Elsevier
Release: 2012-12-02
File: 720 Pages
ISBN-13: 9780323143004

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Analytical Chemistry Has Made Significant Progress In The Last Two Decades. Several Methods Have Come To The Forefront While Some Classical Methods Have Been Relegated. An Attempt Has Been Made In This Edition To Strike A Balance Between These Two Extremes, By Retaining Most Significant Methods And Incorporating Some Novel Techniques. Thus An Endeavour Has Been Made To Make This Book Up To Date With Recent Methods.The First Part Of This Book Covers The Classical Volumetric As Well As Gravimetric Methods Of Analysis. The Separation Methods Are Prerequisite For Dependable Quantitative Methods Of Analysis. Therefore Not Only Solvent Extraction Separations But Also Chromatographic Methods Such As Adsorption, Partition, Ion- Exchange, Exclusion Andelectro Chromatography Have Been Included. To Keep Pace With Modern Developments The Newly Discovered Techniques Such As Ion Chromatography, Super-Critical Fluid Chromatography And Capillary Electrophoresis Have Been Included.The Next Part Of The Book Encompases The Well Known Spectroscopic Methods Such As Uv, Visible, Ir, Nmr, And Esr Techniques And Also Atomic Absorption And Plasma Spectroscopy And Molecular Luminescences Methods. Novel Analytical Techniques Such As Auger, Esca And Photo Accoustic Spectroscopy Of Surfaces Are Also Included.The Final Part Of This Book Covers Thermal And Radioanalytical Methods Of Analysis. The Concluding Chapters On Electroanalytical Techniques Include Potientometry, Conductometry. Coulometry And Voltametry Inclusive Of All Kinds Of A Polarography. The Theme Of On Line Analysis Is Covered In Automated Methods Of Analysis.To Sustain The Interest Of The Reader Each Chapter Is Provided With Latest References To The Monographs In The Field. Further, To Test The Comprehension Of The Subject Each Chapter Is Provided With Large Number Of Solved And Unsolved Problems.This Book Should Be Useful To Those Reads Who Have Requisite Knowledge In Chemistry And Are Majoring In Analytical Chemistry. It Is Also Useful To Practising Chemists Whose Sole Aim Is To Keep Abreast With Modern Developments In The Field.

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Genre:
Author: S M Khopkar
Publisher: New Age International
Release: 1998
File: 500 Pages
ISBN-13: 8122411592

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Genre: Chemistry, Analytic
Author: Douglas A. Skoog
Publisher:
Release: 1965
File: 527 Pages
ISBN-13: UOM:39015015208955

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